Superphanes: Facile and efficient preparation, functionalization and unique properties

نویسندگان

چکیده

Superphanes, compounds in which the two benzene rings clamped parallel on top of each other by six bridges, have been attracting considerable interest because their structural beauty and symmetry. However, progress research superphane chemistry beyond has seriously hampered poor availability. Herein, we report facile scalable synthesis a collection superphanes with diversity unique photophysical properties, as well unusual host–guest behavior. A set secondary amine–linked are obtained via dynamic self–assembly hexakis–amine various readily derived aromatic dialdehyde one pot, followed in–situ reduction NaBH4. Further post–functionalization was exemplified amine to tertiary conversion. All under study were found exhibit interesting fluorescence either solution or solid state. Finally, binding properties stabilization labile 2Cl–·H2O cluster fully protonated 6a both With easy versatile synthesis, modification, reported herein, believe that this offers new possibilities for chemistry, supramolecular host design, advanced functional materials beyond.

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ژورنال

عنوان ژورنال: Tetrahedron chem

سال: 2022

ISSN: ['2666-951X']

DOI: https://doi.org/10.1016/j.tchem.2022.100006